Long-chain hydrocarbons by CO2 electroreduction using polarized nickel catalysts


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Date

2022-06

Publication Type

Journal Article

ETH Bibliography

yes

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Abstract

The electroreduction of CO2, driven by renewable electricity, can be used to sustainably generate synthetic fuels. So far, only copper-based materials have been used to catalyse the formation of multicarbon products, albeit limited to C2 or C3 molecules. Herein, we disclose that inorganic nickel oxygenate-derived electrocatalysts can generate linear and branched C3 to C6 hydrocarbons with sustained Faradaic efficiencies of up to 6.5%, contrasting with metallic nickel, which is practically inactive. Operando X-ray absorption spectroscopy, electrochemical CO stripping and density functional theory pinpoint the presence of stable, polarized Niδ+ active sites associated with Ni–O bonds, which bind CO moderately. The reduction of selected C1 molecules and density functional theory simulations suggest that the Niδ+ sites promote a mechanism reminiscent of the Fischer–Tropsch synthesis: COOH + CHx coupling followed by successive CHx insertions. Our results disclose atom polarization to be the key that prevents the CO poisoning of nickel and enables CO2 reduction to a wider pool of valuable products.

Publication status

published

Editor

Book title

Volume

5

Pages / Article No.

545 - 554

Publisher

Nature

Event

Edition / version

Methods

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Geographic location

Date collected

Date created

Subject

Organisational unit

03871 - Pérez-Ramírez, Javier / Pérez-Ramírez, Javier check_circle
02291 - NCCR Catalysis / NCCR Catalysis

Notes

Funding

ETH-47 19-1 - Microstructured electrocatalysts as a design platform for decentralized ammonia synthesis and carbon dioxide fixation in artificial leaves (ETHZ)
180544 - NCCR Catalysis (phase I) (SNF)

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