Intercomparison Exercise On Fuel Samples For Determination Of Biocontent Ratio By 14c Accelerator Mass Spectrometry
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Date
2023-04
Publication Type
Journal Article
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yes
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Abstract
The method of determining the biobased carbon content in liquid fuel samples is standardized, but different laboratories use different protocols during sample preparation and perform the measurements using different machines. The accelerator mass spectrometry (AMS) laboratories use different combustion, preparation, and graphitization methods for the graphite production for the spectrometric measurements. As a result, the intercomparison between the laboratories is inevitable to prove precision and accuracy and to demonstrate that the results are comparable. In this study, we present the results of an intercomparison campaign involving three C-14 accelerator mass spectrometry laboratories. Five samples were used in the measurement campaign, including two biocomponents (fatty acid methyl ester, hydrotreated vegetable oil), one fossil component (fossil diesel), and two blends (mixtures of fossil and biocomponent with 90-10% mixing ratio) in the laboratories of CEDAD (Italy), ETH (Switzerland), and INTERACT (Hungary). The results presented by the laboratories are comparable, and all three laboratories could determine the biobased carbon content of the samples within 1% relative uncertainty, which is acceptable in the scientific, economic, and industrial fields for biocomponent determination.
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published
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Book title
Journal / series
Volume
65 (2)
Pages / Article No.
539 - 548
Publisher
Cambridge University Press
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Edition / version
Methods
Software
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Date collected
Date created
Subject
AMS; biobased carbon content; liquid fuel; radiocarbon
Organisational unit
08619 - Labor für Ionenstrahlphysik (LIP) / Laboratory of Ion Beam Physics (LIP)