Site-selective C(sp³)–H oxidation of alkyl substrates devoid of functional handles


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Date

2025-03-13

Publication Type

Journal Article

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yes

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Abstract

Although the field of C(sp3)–H oxidation has progressed tremendously over the last decades, the selective oxidation of non-activated positions on hydrocarbon skeletons is still highly challenging. It usually requires the presence of a suitable functional handle in proximity to the desired oxidation site. Here, we present a novel approach to catalyst-directed C–H oxidation that relies on substrate binding via the solvophobic effect in fluorinated alcohols and thus is independent of specific functional groups on the substrate. The supramolecular catalyst Mn(mcp)-RS2 enables the preferential oxidation at the fifth position from the less-hindered side on aliphatic substrates.

Publication status

published

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Book title

Journal / series

Volume

11 (3)

Pages / Article No.

102442

Publisher

Cell Press

Event

Edition / version

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Subject

C–H oxidation; alkanes; solvophobic effect; catalyst control; supramolecular catalyst

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